The synthesis and spectral properties of laser dye doped solid state materials have been reported in this paper . Silica gel based materials that are doped with different concentration of dye synthesized . Porous silica gel based materials have been synthesized by using sol -gel method .TEOS is used as precursor for synthesis work .Many other chemicals are also used in standard concentration for crack free synthesis for these materials . oxazine 170 perchlorate laser dye is used for doping process. Ethanol is used as a solvent for making different concentration of dye solution .The spectral properties of these synthesized silica based SSDL materials were studied with UV Spectrophotometer and their other characteristics are studied by XRD and SEM. From UV Study we have find out the absorbance patterns . Shifting in peaks of absorption spectra has been observed from the data with increase of dye concentration in silica matrix . From XRD studies we have find out about the nature of materials and From SEM we have find the variations in size of particles present in dye doped silica gel particles present in synthesized materials .