A liquid ion exchange joined with the cloud point extraction method is studied to determine Paracetamol in pure form. The method utilizes a liquid ion exchange reaction based upon forming an ion-pair association complex for PAR with Fe(II) in the presence of HCl and nonionic surfactant Triton X-100. The maximum wavelength was 291nm. The optimum condition effect on the separation method was studied: temperature 80°C, heating time 15min., the concentration of Fe(III) was 80µg/mL, and the best surfactant was TritonX-100. The reaction kinetics were studied by using the initial rate method. The calibration curve was linear over the