Metalloorganic compounds of Mn(II), Fe(III), Co(II), Ni(II), Cu(II), Zn(II) and Cd(II) of new diethyl (Z)-4-hydroxy-3-((2-((2-hydroxybenzlidene)amino)phenyl)carbamoyl) benzenesulfonic acid ligand have been synthesized and characterized using spectral analyses; (1H-NMR, mass, IR, UV-VIS and ESR) , magnetic moments , conductance, XRD ,elemental and thermal analysis. Molar conductances in DMF solutions indicated that, the complexes are non-electrolytes;