This experimental investigation reports the impact of boron carbide (B4Cp) particles on Al2214/3%Grp/xB4Cp hybrid metal matrix composites (HMMCs) at a constant weight percentage of Grp (3 wt.%) and x wt.% of B4Cp particles (x = 1.5, 3, 4.5, and 6) produced by a conventional stir casting metallurgical route with bottom pouring facilities. The scanning electron microscope (SEM) combined with the energy dispersive X-ray spectroscope (EDX) shows reasonable uniform distributions of particles in the matrix phase, and a spectrum of elements present in hybrid composites with various intensities. The X-ray diffraction (XRD) analysis was performed for the phase characterization of hybrid composites. Further, the mechanical properties of Al2214 alloy and Al2214/3%Grp/xB4Cp hybrid composites were studied. The experimental results of the hybrid composite revealed improved hardness and tensile properties with the addition of wt.% B4C particles. The tensile fractured surface (SEM) micrographs revealed the root causes and mechanisms of failures in hybrid composites.