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ISSN 2063-5346
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Effect of annealing temperature on the XRD and IR properties of Gd doped nickel ferrites nanoparticles

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Sara Durga Bhavani, A. T. Raghavender, K. Vijaya Kumar, B. Purna Chandra Rao
» doi: 10.48047/ecb/2023.12.si4.944

Abstract

Gd doped nickel ferrites NiFe2−xGdxO4 (0.00  x  0.25) samples were synthesized with solgel method and calcinated at temperatures 700°C, 950°C and 1200°C. With the increase in temperature, we observed the structural changes in the XRD and IR data. With doping Gd content we observed secondary phases in the XRD analysis which has been confirmed with IR analysis. From the XRD and IR experimental observations we confirmed that, the secondary phases might be due to larger ionic radii of Gd compared to Ni ions. The secondary phases observed in all the samples were not able disappear even with the higher annealing temperatures

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